Selecting the Right Oil Analysis Lab - Machinery Lubrication

When you go in for a blood test, do you want to be told what your red and white blood counts are, what your platelet or hemoglobin levels are, or what the mean corpuscular volume is? Unless you’re a medical doctor, probably not.

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You rely on a reputable doctor to analyze the blood count report and tell you if you’re healthy. If he spots concerns, does he say, “You’re unhealthy,” and that’s it? No. You expect him to act with urgency to figure out why you’re not healthy and what can be done to make you better. You expect him to ask a battery of questions to help pinpoint the root causes and explain the problem at hand. That’s why we have doctors and not just blood counts or healthy/unhealthy alarm limits. We need a true diagnostic methodology to help us stay healthy.

Just like blood analysis, oil analysis is undoubtedly complicated. First, someone is tasked with ensuring samples are collected in just the right way to minimize human interference in the results. This requires training. Then, laboratory technicians are rushed to process the sample through a gambit of instruments. They must use precise and consistent methods to avoid the potential interference from such things as previously run samples or variations in sample agitation technique. This calls for a lot of training.

Once the lab tests are completed, the job isn’t finished. You should expect a skilled diagnostician (just like a doctor) to analyze the results, uncover the clues behind the raw data and produce clear recommendations to address any concerns. This last step is probably the most important reason why oil analysis is performed.

It also is arguably the most difficult and often the most overlooked part of it all. This article will offer selection principles necessary to ensure your oil analysis laboratory is giving you what you need to keep your machines healthy.

The End Goal of Oil Analysis

When several end users were asked about the ultimate goal of oil analysis, the most common responses included determining if or when machines were going to fail, detecting incipient machine failures earlier, knowing when to perform an oil change on time, understanding contamination levels and optimizing machine reliability at the lowest possible cost.

While the actual responses varied, a unified answer to the question can be surmised. That is, the end goal of oil analysis is to aid in the optimization of plant-wide reliability by proactively monitoring various indicators within the oil of individual machines. This should be what motivates each plant to design its oil analysis program effectively. This same motivation will also be the deciding factor when evaluating each aspect in selecting and working with a laboratory.

Selection Principles

A laboratory likely will not excel in every aspect of oil analysis as you might hope. In order for it to be competitive, the lab may concentrate its efforts on those areas most valued in the market. The problem is many people are often too focused on price and may unknowingly fall short of their end goal by overlooking some of the most important oil analysis principles.

To capture the scope for evaluating an oil analysis laboratory, selection principles can be grouped into five categories: preparation, regulation, interpretation, communication and evaluation.

1. Preparation

• Sample shipping time/distance to the laboratory
• Provide certified-clean bottles and labels
• Support with sampling methods
• Test slate availability and selection assistance

Preparation includes all things leading up to the laboratory obtaining the oil sample. Choosing a lab that is located close enough to where samples can be delivered within 24 hours or as soon as possible from when the sample was drawn is a must.

The laboratory should supply certified-clean bottles that are selected based on cleanliness targets and the type of oil to be collected. Lab personnel should be knowledgeable about bottle types and when it is appropriate to select one over another.

Along with the bottles, sample labels should be provided requiring the collection of relevant data for the machine, lubricant, environment and maintenance practices. Without this information, the laboratory will not be able to fully interpret the results. The lab may also furnish special packaging materials to facilitate safe and effective shipping of the oil.

If you are new to oil sampling, your laboratory should offer support on the best practices. This will include how often to sample, where to draw a sample and what type of extraction tools should be utilized.

One of the first steps in developing an oil analysis program is understanding which tests should be performed for each equipment class based on the criticality of each machine. This will involve routine testing (potentially performed in-house) and exception testing (for when results come back questionable or abnormal). Your lab should be able to provide the required tests and assistance for optimizing test slates. The more you measure, the more you can analyze and the more potential opportunities ultimately arise.

2. Regulation

• Instrument testing standards validation
• Operating technician certification
• Sample handling process (e.g., agitation)

Most oil analysis test methods are not straightforward but will necessitate having regulations to carefully follow. The regulations may come from standards provided by ASTM, ISO or other comparable standardization organizations. These test standards define the generally accepted procedure, the proper application of the test, the method’s repeatability or reproducibility, calibration requirements and other pertinent data. The laboratory may even choose to follow a modified version of a test standard based on the lab’s preferences. It is critical to understand which standard the lab will use for the required tests as well as the measures taken to ensure the operating technicians are conforming to those standards. There should also be minimum requirements regarding the operating technician’s certifications to perform all necessary tasks within the lab (though outside of the actual test standards).

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The lab’s sample handling processes before and even after the tests are performed will be crucial. Find out how quickly samples are processed for analysis, the sequence of tests and how the remaining sample is stored for potential exception testing. At times, laboratories must take additional steps outside the scope of the testing standards to improve the accuracy of the results, such as the method to effectively agitate the sample prior to analysis or a quick physical inspection of the oil as the initial indicator of a potential concern.

Additionally, each laboratory may decide (and is expected) to go through an extensive self-assessment based on generally accepted standards for maintaining and managing a lubricant testing laboratory. In recent years, ASTM D-12 (Self-Assessment of Quality System Practices in Petroleum Products and Lubricant Testing Laboratories) has been developed to better outline the specific criteria that should be reviewed. If possible, end users should request any documents that can provide the results of laboratory self-assessments and the methodology and criteria that were employed.

3. Interpretation

• Three categories of oil analysis
• Statistical trends and calculations
• Multiple data point correlations
• Maintenance history considerations

If only raw data from the oil analysis tests is presented in the final report, it can be quite confusing and overwhelming for end users who have little to no interpretation experience. To achieve the end goal of oil analysis, there must be a comprehensive interpretation of the data. The interpretation stage can be challenging to summarize, as each oil analysis test provides different forms of data. Nevertheless, some general guidelines should be followed during the interpretation of routine oil analysis.

First, the overall results should focus on verifying or identifying the three oil analysis categories: fluid properties, contamination and wear debris. Second, tests performed on a single sample will not be sufficient to obtain quality results. Developing statistical trends of specific data points and calculations across multiple data points will likely be required to determine if there are any concerns. Perhaps the most important comparison will be against the baseline sample results (new oil test results from the same batch of the used oil result).

The various trends developed for each sample point along with the collected maintenance history and understanding of the machine’s criticality will allow cautionary and critical alarm limits to be set. The lab should offer assistance in establishing these limits, but they must be in agreement with the plant’s overall reliability objectives.

Another thing you must consider is whether your laboratory’s interpreters are familiar with the types of machines from which the oil samples were obtained. If they are not, make sure a specialist is involved to give you the diagnostic skills your machines require. Remember, providing oil analysis data and providing a good explanation of the data are two different things.

4. Communication

• Quality, user-friendly report presentation
• Software integration
• Urgent notification of critical results

After the interpretation has been performed, you should expect your lab to effectively and quickly communicate the results in a quality, user-friendly report. You should see supporting graphs, highlighted concerns, pictures and written interpretations in addition to the complete raw data. In recent years, it’s common for all reports to be routed through a cloud-based software to allow you to easily scan multiple reports and modify charts and trend graphs to suit your needs. The last thing you want is the important details to get lost in the jumble of data or to spend too much time trying to make complex interpretations yourself. While it’s always wise to make your own interpretations (since you are most familiar with your machinery’s history), you don’t want to have to spend an unreasonable amount of time doing so.

Every minute matters when your machines are in distress. Your laboratory should be prepared to immediately contact you if there are any critical concerns. This may be via call, text, or whatever method works best for you. When it comes to these critical notifications, do not rely on the standard delivery methods for your oil analysis results, as you may overlook their urgency. For example, if you normally receive all oil analysis results by , you may not perceive the urgency of an about a critical concern because it might be seen as a typical report in your inbox, likely delaying its review.

5. Evaluation

• Exception test recommendations
• Root cause investigation
• Assess other condition monitoring results
• Customer-focused support

After critical alarms are triggered and urgent notifications are sent, subsequent communication from the lab should help you evaluate the problem at hand and make quick decisions. The laboratory should assist you in determining exception tests that could provide more information about any concern identified by a routine test. This further analysis should include techniques like microscopic analysis, which can be obtained from any remaining oil from the original sample. More oil may also need to be drawn from the machine. These exception tests are intended to confirm, deny or provide more details in order to find the root cause of the issue. With this data and more in-depth examination into the recent events of the machine’s operating conditions, investigation reports and other condition monitoring technologies, remediation recommendations can be formulated.

In many cases, the laboratory may be able to provide the investigative assistance you need to get to the root cause of a potential failure. Know your lab’s full capabilities and set your expectations accordingly. The laboratory should be passionate about detecting and solving problems, and share your end goal of aiding in the optimization of plant-wide reliability by proactively monitoring various indicators within the oil of individual machines.

At What Cost?

Each of these oil analysis selection principles can be refined by considering the optimum reference state (ORS) of each machine or, more importantly, your plant’s overall reliability objectives. If price was not a concern, you would simply choose a lab that could deliver on all of these principles. Unfortunately, price eventually must be a concern.

So when does the price of oil analysis outweigh its returns? First, you must consider the impact of a potential failure for any of your machines, including the resulting cost of parts, labor and lost revenue from a production interruption. Then, depending on the magnitude of this impact, you must decide how much you would be willing to spend to avoid the average incident, regardless of whether there is a history of failure. In almost every circumstance, a single catch that avoids the average failure would more than justify the typical cost of an oil analysis program for an entire plant.

Oil analysis services are generally competitively priced in the market. Nevertheless, beware of the potential shortcomings of very low-cost or even free oil analysis programs, such as those provided by a lube supplier. Even if the oil analysis is free, it still costs you time and money to collect samples and manage results. If the oil analysis program isn’t created with your end goal as the focus, you may not be giving yourself any sort of advantage. You may be better off spending a few extra dollars to guarantee you get the value you’re trying to achieve. Asking the questions specified by the selection principles will help ensure this. As the optimum reference state suggests, there is an optimum effectiveness zone that is a balance between the cost of an investment (like oil analysis) and the cost of unreliable operation. The total cost of reliability will be the lowest at this optimum effectiveness zone.

So while price must be taken into consideration, it should not be your top priority. Consider price only after you can verify your satisfaction with the level of service and quality the lab offers in each of the selection principles as it relates to your end goal. Like most things, it is often a tradeoff between price, service and quality, where two of the three are achievable at a desired level. Do not sacrifice the necessary levels of service and quality for price. The attainment of your end goal is depending on it.

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Hi,

For years I've done regular oil analysis for my engines, trans and gen.

For many years I used a firm local to me in the SF bay area - until they were bought out and customer service became an unknown concept.

For about 2 years I've been using Blackstone Labs. I mostly like their services, the analysis reports and the pricing is reasonable. However, for about 6 months they've been taking longer and longer to turn results around... I fear that they are a victim of their own success.

For my last samples with them, it has taken 1 month+ (after they get the sample) for them to provide lab results. That's too long for my needs.

Does anyone have a recommendation for an oil analysis lab that reliably returns results (preferably in about a week) after they receive the sample? Yes, I've noticed Blackstone is taking longer for their oil analysis. For me it's not an issue as it's just routine testing. There are times I'm changing and sampling the oil every 2 weeks, so not a big deal.

My recommendation would be to call them and see if you can get faster turnaround without an increased price. I would imagine there would have to be customers who need faster service without it being critical.

Ted

Hi,

For years I've done regular oil analysis for my engines, trans and gen.

For many years I used a firm local to me in the SF bay area - until they were bought out and customer service became an unknown concept.

For about 2 years I've been using Blackstone Labs. I mostly like their services, the analysis reports and the pricing is reasonable. However, for about 6 months they've been taking longer and longer to turn results around... I fear that they are a victim of their own success.

For my last samples with them, it has taken 1 month+ (after they get the sample) for them to provide lab results. That's too long for my needs.

Does anyone have a recommendation for an oil analysis lab that reliably returns results (preferably in about a week) after they receive the sample?

I do believe that all of the labs use mostly the same equipment to analyze oil. In other words, one house is as good as another. What I do not like about Blackstone is that they charge extra for TBN analysis. TBN is a critical measure of a diesel oil's continued efficacy. If the TBN is of sufficient amount and the viscosity is within range, the oil can continue to be used, quite safely.

I do believe that all of the labs use mostly the same equipment to analyze oil. In other words, one house is as good as another. What I do not like about Blackstone is that they charge extra for TBN analysis. TBN is a critical measure of a diesel oil's continued efficacy. If the TBN is of sufficient amount and the viscosity is within range, the oil can continue to be used, quite safely.

While TBN analysis is valuable to a point for determining the time or mileage period of routine oil changes, regular oil analysis is more focused on wear metals, antifreeze and water contamination, oil viscosity, and fuel trace percentages, atleast for Dino based oils.

Ted

While TBN analysis is valuable to a point for determining the time or mileage period of routine oil changes, regular oil analysis is more focused on wear metals, antifreeze and water contamination, oil viscosity, and fuel trace percentages, atleast for Dino based oils.



Ted

Ted, agree 100%, but if one extends oil change periods because the oil is still good to use, would not the wear analysis still be just as useful when next tested? Wear elements are not measured in absolute terms, they are measured against the numbers of hours the lube has been used, so, if the TBN is in range and the viscosity is within range, then why not continue to use good oil? Continue to test at regular intervals and you will still have a history, and an indicator of antifreeze, water, or fuel dilution. Dirty oil? That is what the "soot" measure is for. Just change the filter and carry on. In no way was I suggesting that regular testing should not be done, dino or synthetic.

Ted, agree 100%, but if one extends oil change periods because the oil is still good to use, would not the wear analysis still be just as useful when next tested? Wear elements are not measured in absolute terms, they are measured against the numbers of hours the lube has been used, so, if the TBN is in range and the viscosity is within range, then why not continue to use good oil? Continue to test at regular intervals and you will still have a history, and an indicator of antifreeze, water, or fuel dilution. Dirty oil? That is what the "soot" measure is for. Just change the filter and carry on. In no way was I suggesting that regular testing should not be done, dino or synthetic.

I have no first hand experience with synthetic oils. My experience with traditional motor oil is that over time, wear metal numbers significantly increase in a non linear fashion. In essence, wear metals in the oil increase the production of other wear metals. As a result, there is a balancing act between useful remaining life of oil versus increasing concentration of abrasive wear metals. As I tend to rack the hours up (6,000 Hr. In 8 years), I choose reduced wear over reduced cost of oil changes.

As a side note, I regret not having added a supplemental oil filter with a much finer filtration system when installing this engine. The savings in oil changes would have easily paid for the system.

Ted

I would have recommended Herguth Labs in Vallejo, but they were just sold to SGS and I know nothing of them. Maybe someone else is familiar with them.

Hergurth is who I used to use. When they got bought by SGS I started having problems with them. Example: SGS required a new account set up and would not link the Herguth reports from before to the new account - so the sample history was hard to access (I had to log into the old account to see those). Several other problems with SGS re purchasing sample kits etc contributed to my decision to go to Blackstone. Since the history chain was already broken, it was a opportune time to restart elsewhere. FYI, I used Blackstone, and have for decade or two. They do seem to take longer than they used too, but I don't really care since the reports are pretty consistent. I have had some very educational communications with Blackstone over the years, and I suspect if I really needed a sample tested quickly, I could ask and they would bump me up in line.

I like it that they keep a number of my old tests in the report so I can see what has been happening over quite a few samples without having to find my old reports.

Later,
Dan I have used www.eoilreports.com/login and have had several issues with them, such as mixing samples from other customers and making changes to equipment or data. I would not recommend them; however, I do like the reports and timeliness. I have used Blackstone and will not after a 6 week wait. What if there was a significant problem with a result and I just added more damage to equipment because of a sample waiting on a shelf waiting to be analyzed. Thanks to everyone for the leads to other oil analysis firms.

I think at the next sample interval, I'll pull 2-4 samples at the same time and send each to different labs. That will let me compare the reports and the customer service levels. I realize that will require a small investment cost for the multiple analysis.
The current situation with Blackstone is that it's taking 5+ weeks to get a report (from day of sample shipment to report available).

In some situations that's OK, but not for my current needs.


I had a trans cooler start to fail and a trans' ATF got contaminated. Many flushes later I'm close (I hope) to a normal analysis report. I'm down to running for about 20 hrs and then sampling to see if the atf change cycle can end. I can't handle that cycle time being 5-6 wks long just due to the lab lead time.

Other than the long turnaround times lately, there are many reasons I like Blackstone. Not the least is that a real person answers their and they are always nice, polite and helpful. They are just currently running a big back log. I wonder if a conversation in advance with Blackstone (or whomever) could arrange an expedited analysis and reports?

I just checked our last previous sample/report time. I sent both on 11/06. Got stbd report on 11/23. Nil heard about port for a while, so I queried them on 11/27 and they confirmed sample receipt on 11/29. I got their port report on 12/1.

Part of the was my fault; I'd mis-typed my CC number on the form for port engine. Otherwise, I didn't think much about the elapsed time for the whole process. And that was a couple years ago, anyway...

-Chris So I sent off an to Blackstone a few days ago regarding the increasing length of time for reports. Received the following response:

Good morning Ted,

We appreciate you bringing this to our attention. Yes- we are aware
many of our customers are frustrated with our turn around time. We're
doing our best to expand our very small business, creating another
lab, hiring more workers, but training takes time. We do always offer
the option to over-night a sample to us. We typically get those done
in 2-4 business days. Please let us know if you need anything else.

Thanks,
The Blackstone Team

Ted